This is a page describing data taken during an experiment at the ISIS Neutron and Muon Source. Information about the ISIS Neutron and Muon Source can be found at https://www.isis.stfc.ac.uk.
Order and disorder in sodium amide
Abstract: Sodium amide has recently attracted interest as a catalyst for the decomposition of ammonia as a means of producing hydrogen. As such, its properties are of increasing relevance to the design and optimisation of sodium amide-based catalyst systems. We have previously observed interesting structural properties in solid sodium amide, including significant disorder in the amide units, even at room temperature. In this proposal, we request two days of access on the SANDALS instrument to measure the diffraction of a sample of sodium amide in order to gain insight into the disorder in the structure as a function of temperature, including the transition from solid to the melt.
Principal Investigator: Professor Bill David
Experimenter: Dr Sam Callear [Deactivated]
Experimenter: Dr Josh Makepeace
DOI: 10.5286/ISIS.E.RB1510632
ISIS Experiment Number: RB1510632
Part DOI | Instrument | Public release date | Download Link |
---|---|---|---|
10.5286/ISIS.E.61784388 | SANDALS | 17 June 2018 | Download |
10.5286/ISIS.E.61002348 | SANDALS | 17 June 2018 | Download |
Publisher: STFC ISIS Neutron and Muon Source
Data format: RAW/Nexus
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Data Citation
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[author], [date], [title], [publisher],
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Professor Bill David et al; (2015): Order and disorder in sodium amide, STFC ISIS Neutron and Muon Source, https://doi.org/10.5286/ISIS.E.RB1510632
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