ISIS Neutron and Muon Source Data Journal

This is a page describing data taken during an experiment at the ISIS Neutron and Muon Source. Information about the ISIS Neutron and Muon Source can be found at https://www.isis.stfc.ac.uk.


Order and disorder in sodium amide

Abstract: Sodium amide has recently attracted interest as a catalyst for the decomposition of ammonia as a means of producing hydrogen. As such, its properties are of increasing relevance to the design and optimisation of sodium amide-based catalyst systems. We have previously observed interesting structural properties in solid sodium amide, including significant disorder in the amide units, even at room temperature. In this proposal, we request two days of access on the SANDALS instrument to measure the diffraction of a sample of sodium amide in order to gain insight into the disorder in the structure as a function of temperature, including the transition from solid to the melt.

Principal Investigator: Professor Bill David
Experimenter: Dr Sam Callear [Deactivated]
Experimenter: Dr Josh Makepeace

DOI: 10.5286/ISIS.E.RB1510632

ISIS Experiment Number: RB1510632

Part DOI Instrument Public release date Download Link
10.5286/ISIS.E.61784388 SANDALS 17 June 2018 Download
10.5286/ISIS.E.61002348 SANDALS 17 June 2018 Download

Publisher: STFC ISIS Neutron and Muon Source

Data format: RAW/Nexus
Select the data format above to find out more about it.

Data Citation

The recommended format for citing this dataset in a research publication is as:
[author], [date], [title], [publisher], [doi]

For Example:
Professor Bill David et al; (2015): Order and disorder in sodium amide, STFC ISIS Neutron and Muon Source, https://doi.org/10.5286/ISIS.E.RB1510632

Data is released under the CC-BY-4.0 license.



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